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(a) 1 H NMR (D 2 O, 600 MHz, 80 °C) of β-CD, CDP, CDPC-3, -5, and -10. 1 H– 13 C HSQC spectra (D 2 O, 600 MHz, 80 °C) of (b) CDP, (c) CDPC-5, and (d) CDPC-10. (e) The chemical structure of CDPC is provided to assist in the spectra interpretation.

Journal: Biomacromolecules

Article Title: Cyclodextrin–Epichlorohydrin–Cyanoguanidine Polymer for Resveratrol Delivery to Enhance Human Chondrocyte Function in Cartilage Repair

doi: 10.1021/acs.biomac.5c02392

Figure Lengend Snippet: (a) 1 H NMR (D 2 O, 600 MHz, 80 °C) of β-CD, CDP, CDPC-3, -5, and -10. 1 H– 13 C HSQC spectra (D 2 O, 600 MHz, 80 °C) of (b) CDP, (c) CDPC-5, and (d) CDPC-10. (e) The chemical structure of CDPC is provided to assist in the spectra interpretation.

Article Snippet: β-Cyclodextrin (β-CD) was purchased from Cyclolab R&D Ltd. (Budapest, Hungary).

Techniques:

Schematic Representation of the Reaction of β-CD and CyG in the Presence of ECH toward the Formation of CDPC; (a,b) Illustrate Two Proposed Formation Mechanisms and Representative Intermediates in the Condensation of β-CD, ECH, and CyG. (a) CyG Incorporated within the Polymer Backbone and (b) CyG Positioned at the Terminal End

Journal: Biomacromolecules

Article Title: Cyclodextrin–Epichlorohydrin–Cyanoguanidine Polymer for Resveratrol Delivery to Enhance Human Chondrocyte Function in Cartilage Repair

doi: 10.1021/acs.biomac.5c02392

Figure Lengend Snippet: Schematic Representation of the Reaction of β-CD and CyG in the Presence of ECH toward the Formation of CDPC; (a,b) Illustrate Two Proposed Formation Mechanisms and Representative Intermediates in the Condensation of β-CD, ECH, and CyG. (a) CyG Incorporated within the Polymer Backbone and (b) CyG Positioned at the Terminal End

Article Snippet: β-Cyclodextrin (β-CD) was purchased from Cyclolab R&D Ltd. (Budapest, Hungary).

Techniques: Polymer

DOSY spectra (D 2 O, 600 MHz, 25 °C) of β-CD, CDP, and CDPC-5. The x -axis represents the 1 H chemical shift of the samples in D 2 O, while the y -axis corresponds to the diffusion dimension. The 1 H signal assignments are included in the spectra.

Journal: Biomacromolecules

Article Title: Cyclodextrin–Epichlorohydrin–Cyanoguanidine Polymer for Resveratrol Delivery to Enhance Human Chondrocyte Function in Cartilage Repair

doi: 10.1021/acs.biomac.5c02392

Figure Lengend Snippet: DOSY spectra (D 2 O, 600 MHz, 25 °C) of β-CD, CDP, and CDPC-5. The x -axis represents the 1 H chemical shift of the samples in D 2 O, while the y -axis corresponds to the diffusion dimension. The 1 H signal assignments are included in the spectra.

Article Snippet: β-Cyclodextrin (β-CD) was purchased from Cyclolab R&D Ltd. (Budapest, Hungary).

Techniques: Diffusion-based Assay

ABTS •+ scavenging activity expressed in % for β-CD, CDP, and CDPC-5, with different concentrations from 0.12 to 0.48 mg·mL –1 , and for CDP/RES and CDPC-5/RES with concentrations of 0.12 mg·mL –1 .

Journal: Biomacromolecules

Article Title: Cyclodextrin–Epichlorohydrin–Cyanoguanidine Polymer for Resveratrol Delivery to Enhance Human Chondrocyte Function in Cartilage Repair

doi: 10.1021/acs.biomac.5c02392

Figure Lengend Snippet: ABTS •+ scavenging activity expressed in % for β-CD, CDP, and CDPC-5, with different concentrations from 0.12 to 0.48 mg·mL –1 , and for CDP/RES and CDPC-5/RES with concentrations of 0.12 mg·mL –1 .

Article Snippet: β-Cyclodextrin (β-CD) was purchased from Cyclolab R&D Ltd. (Budapest, Hungary).

Techniques: Activity Assay